Department Urban Water Management

MS2field

Transfer to trailer

October 2018.  We thought we had thought of everything. For a variety of issues we had to think and rethink multiple times to find practical and robust solutions:

  • On the one hand, everything needs to be fixed and tightened to not move while driving.
  • On the other hand, how to make all parts easily accessible for maintenance, e.g. the filtration device in the source water bypass?
  • How to facilitate appropriate heating and cooling?
  • How to guarantee a safe atmosphere inside the trailer (solvents, nitrogen generator)?
  • How to prevent flooding of the trailer in case of pipe burst, or avoid the latter?
  • How to guarantee power supply and remote control of all safety relevant components?
  • How to minimize impact of vibrations?

We are enormously thankful for the support we received from our colleagues internally (many technical solutions and advice on design of remote control) and externally (plumbing and electricity)!

Now the MS is operating in the trailer and we are performing first prolonged measurements on water from the nearby creek (Chriesbach).

 

 

Short making-of video:

First success

May 2018.  In March and April, we carried out more preliminary tests and optimized the sample preparation. And most recently, the system succeeded in measuring more than 500 samples over a one-week period – one every 20 minutes – with minimal human interaction, resulting in a dataset of 500 raw files (35 GB, 2 x 10e6 scans). Pre-processing (peak picking and alignment) resulted in 90,000 time series that we evaluated with spectral analysis (periodograms). We identified approx. 50 interesting clusters. One example is a set of 38 profiles that show a distinct diurnal pattern MON-FRI but do not occur on SAT and SUN.

Assembling parts

February 2018.  The MS arrived in January. We assembled all required components in our experimental hall and tested the new workflow with “primary clarifier effluent”. Six months after the project start and just one month after the instrument arrived, we have a basic setup that seems to fulfil our requirements: a powerful pump to deliver a sample stream, a robust filtration unit, a versatile sample preparation unit, different options for front ends and a laboratory mass spectrometer that seems to cope well with conditions that are more variable than in a normal laboratory. Now we are performing first measurements with real sewage (“sand trap effluent”) and are looking for a suitable trailer.

First three months

November 2017.  Project start in September 2017! Many small details that are not an issue or easy to solve in a laboratory, require special attention and special solutions when aiming for operating an unattended system in a remote location over an extended period.

Our vision

2016/17.   Wouldn’t it be interesting to measure a broad suite of micropollutants at high temporal resolution to better understand their occurrence and fate? Do you know a system that can take hundreds of samples a week for multiple weeks, and do you have the capacity to analyse them in a lab? We don’t.

Therefore, we seek collaboration with industry partners and apply for discretionary funding. Together with Thermo and CTC, our ambitious goal* is to measure micropollutant concentrations at intervals of minutes to hours, and quantify them directly in the field – with the same, high quality as traditionally in the lab.

* A goal is a dream with a deadline - Napoleon Hill (1883-1970), author in the area of the new thought movement, one of the great writers on success.

Project Team

Dr. Michael StravsPostdoctoral scientistTel. +41 58 765 6742Send Mail
Heinz SingerSenior scientist / group leaderTel. +41 58 765 5577Send Mail
Dr. Christian StammTel. +41 58 765 5565Send Mail
Dr. Christoph OrtGroup LeaderTel. +41 58 765 5277Send Mail

Duration

September 2017  -  August 2019

Financing

Eawag  -  Discretionary Funding